Polymers · Section 113 of 116

Addition polymers

Practice this — interactive lesson

An addition polymer comes from an alkene, and the mechanism is the electrophilic or radical addition you already know, repeated. Nothing is lost, so the repeat unit has exactly the same formula as the monomer — which is the quickest way to recognize one.

The chain reaction, in three stages

Radical polymerization is the commonest, and it is a chain reaction with the three stages any chain reaction has:

Because termination needs two radicals to find each other in a solution where they are very dilute, propagation runs a long way first. That is why chains are long.

This is the same initiation–propagation–termination structure as radical halogenation, and it is worth seeing the two as one mechanism. The difference is only what the radical adds to: a C–H bond there, a C=C bond here.

Head-to-tail, and why

Take a monosubstituted alkene, CH2=CHX. The growing radical can add to either carbon, and it adds to the CH2 end — because that leaves the radical on the substituted carbon, which is the more stable of the two.

Do that repeatedly and every substituent ends up on alternate carbons, which is called head-to-tail linking. It is the same regiochemical argument as Markovnikov's rule, reached by asking which intermediate is more stable rather than by quoting a rule.

The polymers worth recognizing

MonomerPolymerWhere you meet it
Ethylene, CH2=CH2PolyethyleneBags, bottles, pipe
Propylene, CH2=CHCH3PolypropyleneRope, containers, carpet
Vinyl chloride, CH2=CHClPVCPipe, flooring, insulation
Styrene, CH2=CHPhPolystyrenePackaging, foam cups
Tetrafluoroethylene, CF2=CF2PTFE (Teflon)Non-stick coatings
Methyl methacrylatePMMA (Plexiglas)Transparent sheet

Every one of these is drawn the same way. Take the monomer, break the π bond, and write the repeat unit in brackets with a bond out of each side: –[CH2–CHX]–n.

Tacticity: the same polymer, three materials

In a monosubstituted polymer such as polypropylene, every substituted carbon in the chain has a definite orientation — the substituent points to one side or the other — so the arrangement along the chain matters. (These are not stereocenters in the CIP sense: the two chain directions are near-identical, which is exactly why tacticity gets its own vocabulary instead of R and S. Polyethylene and PTFE have no such centers at all, and no tacticity.) Three patterns have names:

Radical polymerization gives atactic polymer, because a planar radical has no preference about which face the next monomer arrives on. Getting isotactic polypropylene — the useful kind — needs a Ziegler–Natta catalyst, which holds the growing chain on a metal center and forces each addition to happen the same way. Atactic polypropylene is a sticky goo; isotactic polypropylene is rope and car bumpers. Same repeat unit.

Branching, and the two polyethylenes

linear — chains touch along their lengthHDPE: crystalline, dense, rigidmilk bottles and pipebranched — held apartLDPE: less crystalline, less dense, floppyplastic bagsSame monomer. Same repeat unit. Same molecular formula.The difference is architecture, and it is the whole material.
The two polyethylenes. High-pressure radical polymerization lets a growing chain abstract a hydrogen from itself and continue from there, leaving branches; a Ziegler–Natta catalyst holds the chain end and suppresses it. Branches stop the chains touching, and everything else follows.This is the fatty-acid argument from the biomolecules chapter, applied to a different molecule. Straight chains lie against their neighbors along their full length and the London forces add up; a bend or a branch breaks that contact and the melting point falls with it. Tacticity does the same job by a different route — atactic polypropylene cannot pack either, and it is a goo where the isotactic polymer is rope.

A growing radical sometimes abstracts a hydrogen from its own chain a few carbons back, and the chain then continues from there — leaving a branch. Radical polymerization of ethylene at high pressure does this constantly, giving low-density polyethylene: branched, poorly packed, flexible, the stuff of plastic bags.

A Ziegler–Natta catalyst suppresses it, giving high-density polyethylene: linear, well packed, rigid, the stuff of milk bottles and pipe. Identical repeat unit, identical formula, different architecture, and genuinely different materials.

What carries forward

Initiation, propagation, termination; head-to-tail regiochemistry from the more stable radical; and two structural variables — tacticity and branching — that change the material without changing the chemistry. When a question gives you an alkene and asks for the polymer, break the π bond and bracket the repeat unit; when it gives you two materials with the same formula, the answer is architecture.